Date of Completion

9-9-2013

Embargo Period

9-9-2013

Keywords

meso-tetrakis(pentafluorophenyl)porphyrin, meso-tetraphenylporphyrin, Cyanide sensing, High pH sensing, Fragmentation Patterns, Axial imidazole binding strengths, Carbonyl stretching frequency

Major Advisor

Dr. Christian Brueckner

Associate Advisor

Dr. Steven Suib

Associate Advisor

Dr. Edward Neth

Associate Advisor

Dr. Alfredo Angeles-Boza

Associate Advisor

Dr. James Bobbitt

Field of Study

Chemistry

Degree

Doctor of Philosophy

Open Access

Open Access

Abstract

This thesis describes in a number of separate chapters a range of studies that measure the variation of specific physical properties with structural modification of the macrocycles, with a particular focus also on using their coordinated metals as probes. Specifically, the transition metal ions are used as tools for interrogation of the electronic properties of porphyrins and pyrrole-modified porphyrins. With the aim of better understanding the electronic and structural factors that govern the optical responses, axial binding strengths, fragmentation patterns and carbonyl stretching frequencies of meso-tetraarylporphyrins, a rational design of pyrrole-modified metalloporphyrins with designed optical properties is derived.

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